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This episode focuses on the intricacies of preparing and analyzing samples containing niobium and tantalum, two elements with similar geochemistry and behavior. Learn effective methods for dissolving metals, alloys, and oxides using techniques such as HF stabilization and fusion methods, while addressing challenges like signal quenching and purity issues. Discover best practices for ICP-OES and ICP-MS testing, including how to manage interferences from tungsten and rare earth oxides. This episode is packed with actionable insights for anyone working with these unique and often tricky elements.

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In this episode, we explore the versatile and "colorful" chemistry of vanadium in sample preparation and analysis. Learn about effective methods for dissolving vanadium metals, alloys, and oxides, including tips on handling its various oxidation states. Discover practical advice for working with vanadium in different matrices, stability insights, and unique color-change indicators that can help you assess sample prep success. With vanadium being straightforward to test on ICP-OES and ICP-MS, this episode highlights everything you need to achieve reliable results with this stable element.

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This episode explores best practices for preparing and analyzing samples containing zirconium and hafnium. Discover the unique challenges these "geochemical twins" present, from handling metals and oxides with HF to using sodium carbonate and tetraborate fusions. Learn how to maintain stability in solution and avoid common ICP interferences, especially when working with trace elements. Perfect for labs tackling complex matrices, this episode offers essential insights for reliable results in zirconium and hafnium analysis.

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This episode covers essential methods for handling titanium in sample prep and analysis, from dissolving titanium alloys and oxides to stabilizing it in solution. Explore the unique challenges of working with titanium, including the need for careful HF handling and tips for preventing hydrolysis. Discover effective techniques for ICP-OES and ICP-MS testing, along with ways to navigate common interferences from elements like scandium and vanadium. This guide will help labs ensure accuracy and stability in titanium analysis, making it a valuable resource for both novice and experienced analysts.

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This episode delves into the complexities of preparing and analyzing samples containing thorium and uranium. Learn how to effectively dissolve metal and oxide samples and explore stability challenges related to HF sensitivity and acid compatibility. We also cover essential ICP-OES and ICP-MS testing strategies, including handling uranium isotopes and understanding the nuances of depleted versus natural uranium sources. Whether you're ensuring accurate results in ICP analysis or navigating radioactive materials, this episode provides valuable insights to enhance your lab's capabilities.

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In this episode, our experts tackle the complexities of working with rare earth elements, from sample prep to interference correction. Listen as they explore methods for dissolving rare earth samples and maintaining stability in solution. The team also delves into the challenges of analyzing rare earths using ICP-OES and ICP-MS, including tips for mitigating oxide interferences and selecting optimal isotopes. Perfect for those dealing with high-purity rare earth samples or navigating their rich spectra, this episode is packed with essential insights for accurate analysis.

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In this episode, we focus on scandium, a key element used frequently as an internal standard in ICP analysis. The team dives into important considerations for keeping scandium stable in solution and avoiding HF sensitivity. They also discuss testing strategies using both ICP-OES and ICP-MS, including how to manage potential spectral interferences and optimize your setup for accurate results. Whether you work with scandium regularly or are looking to fine-tune your techniques, this episode offers essential insights to help you succeed in the lab.

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This week, the team discusses the preparation and analysis of samples containing strontium and barium. Discover the similarities between these elements and calcium, from solubility tips to handling HF sensitivity and sulfate contamination risks. The team also provides insights into testing with ICP-OES and ICP-MS, highlighting key interferences to watch for and ways to improve detection limits.

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